An efficient acetylation of primary and secondary aliphatic alcohols with acetic anhydride in the presence of graphite bisulphate

Secen H., KALPAR A.

TURKISH JOURNAL OF CHEMISTRY, cilt.23, sa.1, ss.27-30, 1999 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 23 Sayı: 1
  • Basım Tarihi: 1999
  • Dergi Adı: TURKISH JOURNAL OF CHEMISTRY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, TR DİZİN (ULAKBİM)
  • Sayfa Sayıları: ss.27-30
  • Anahtar Kelimeler: primary and secondary aliphatic alcohols, acetic anhydride, graphite bisulphate, acetylation
  • Atatürk Üniversitesi Adresli: Evet

Özet

In cyclohexane, thirteen examples of primary and secondary aliphatic alcohols were easily converted to the corresponding acetate derivatives within a short time, ranging from 5 min to 2.5 h, and in good yields close to 90 %, using acetic anhydride as reagent and graphite bisulphate as an efficient catalyst.