MATERIALS CHARACTERIZATION, cilt.46, sa.4, ss.311-316, 2001 (SCI-Expanded)
The mechanical and structural properties of TiN-coated, plasma-nitrided and TiN coated-nitrided AISI 8620 steel were investigated. The plasma nitriding process was carried out under various conditions of temperature (500 degreesC), time (1, 4, 10 h), and gas mixture (70% N-2 + 30% H-2) at 10-mbar working pressure. The titanium nitride coatings were deposited using a closed-field unbalanced magnetron sputtering system (CFUBMS). Nitrided, TiN-coated and TiN+nitrided sample surface were characterized using microhardness tests, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The highest microhardness (10 gf) was obtained at 500 degreesC for 4 h nitriding time. The alloy nitrides produced (CrN, Mn4N) showed a stable condition at all nitriding times. The adhesion of nitrided+TiN coated sample was obtained at 4 h using a plasma-nitrided process. (C) 2001 Elsevier Science Inc. All rights reserved.