One-pot Electrochemical Synthesis of Ni Nanoparticles-Decorated Electroreduced Graphene Oxide for Improved NADH Sensing

Urhan B. K., Dogan H., Ozer T., Demir U.

ELECTROANALYSIS, cilt.32, sa.10, ss.2323-2329, 2020 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 32 Sayı: 10
  • Basım Tarihi: 2020
  • Doi Numarası: 10.1002/elan.202060117
  • Dergi Adı: ELECTROANALYSIS
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, Aerospace Database, Applied Science & Technology Source, BIOSIS, Chimica, Communication Abstracts, Metadex, Civil Engineering Abstracts
  • Sayfa Sayıları: ss.2323-2329
  • Anahtar Kelimeler: Electrooxidation of NADH, Electrochemical reduction, reduced graphene oxide, NADH sensing, Ni nanoparticles, PASTE ELECTRODE, NICKEL-OXIDE, REDUCTION, PERFORMANCE, COMPOSITE, FACILE, FILMS
  • Atatürk Üniversitesi Adresli: Evet

Özet

Ni nanoparticles (NPs) decorated electrochemical reduced graphene oxide (NiNPs/ERGO) nanocomposites (NCs) on ITO electrode were successfully fabricated using one-pot simultaneously electrochemical co-reduction method at room temperature. The NiNPs/ERGO electrodes demonstrated very good electrocatalytic activity in the oxidation of NADH at a low oxidation potential (similar to+430 mV), a wide linear range (1-500 mu M), a calculated detection limit of 0.002 mu M. Compared to ERGO and NiNPs electrodes, the synthesized NiNPs/ERGO NCs have high electrocatalytic activity due to synergistic effect emerged between NiNPs and ERGO. The results indicated that the NiNPs/ERGO NCs can be easily prepared by one-pot electrochemical technique and NiNPs/ERGO could used to as potential biosensor for the NADH detection.